Carbamic acid, [2-chloro-5-(4,4-diethoxy-2-methyl-1-butenyl)-3-methoxyphenyl]methyl-, methyl ester, (E)-

Base Information

Chemical Name:Carbamic acid, [2-chloro-5-(4,4-diethoxy-2-methyl-1-butenyl)-3-methoxyphenyl]methyl-, methyl ester, (E)-
CAS No.:141206-85-1
Molecular Formula:C₁₉H₂₈ClNO₅
Molecular Weight:385.888
Hs Code.:

Synonyms:

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Chemical Property of Carbamic acid, [2-chloro-5-(4,4-diethoxy-2-methyl-1-butenyl)-3-methoxyphenyl]methyl-, methyl ester, (E)-

Chemical Property:

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Technology Process of Carbamic acid, [2-chloro-5-(4,4-diethoxy-2-methyl-1-butenyl)-3-methoxyphenyl]methyl-, methyl ester, (E)-

There total 10 articles about Carbamic acid, [2-chloro-5-(4,4-diethoxy-2-methyl-1-butenyl)-3-methoxyphenyl]methyl-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6635-20-7
isonitrovanillin

: 141206-85-1,141206-86-2
[2-Chloro-5-((Z)-4,4-diethoxy-2-methyl-but-1-enyl)-3-methoxy-phenyl]-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 72 percent / LiCl, p-toluenesulphonyl chloride, HMPA / 80 °C / 1.) 18 h, 2.) 4 h

2: 100 percent / p-toluenesulphonic acid / benzene / 16 h / Heating

3: 99 percent / H₂NNH₂*H₂O, Raney Ni / ethanol / 0.67 h / Ambient temperature

4: 99 percent / pyridine / 2 h / Ambient temperature

5: 99 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

6: 100 percent / 1N aq. HCl / acetone / 1.5 h / Ambient temperature

With pyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; nickel; sodium hydride; toluene-4-sulfonic acid; hydrazine hydrate; p-toluenesulfonyl chloride; lithium chloride; In tetrahydrofuran; ethanol; acetone; benzene;
DOI:10.1016/S0040-4020(01)88513-6

Reference yield:

: 83163-84-2
4-Chloro-3-methoxy-5-nitro-benzaldehyde

: 141206-85-1,141206-86-2
[2-Chloro-5-((Z)-4,4-diethoxy-2-methyl-but-1-enyl)-3-methoxy-phenyl]-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / p-toluenesulphonic acid / benzene / 16 h / Heating

2: 99 percent / H₂NNH₂*H₂O, Raney Ni / ethanol / 0.67 h / Ambient temperature

3: 99 percent / pyridine / 2 h / Ambient temperature

4: 99 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

5: 100 percent / 1N aq. HCl / acetone / 1.5 h / Ambient temperature

With pyridine; hydrogenchloride; nickel; sodium hydride; toluene-4-sulfonic acid; hydrazine hydrate; In tetrahydrofuran; ethanol; acetone; benzene;
DOI:10.1016/S0040-4020(01)88513-6

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 141206-85-1,141206-86-2
[2-Chloro-5-((Z)-4,4-diethoxy-2-methyl-but-1-enyl)-3-methoxy-phenyl]-methyl-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 88 percent / HNO₃ / diethyl ether / 1.) 10 deg C, 2.) rt, 4 h

2: 72 percent / LiCl, p-toluenesulphonyl chloride, HMPA / 80 °C / 1.) 18 h, 2.) 4 h

3: 100 percent / p-toluenesulphonic acid / benzene / 16 h / Heating

4: 99 percent / H₂NNH₂*H₂O, Raney Ni / ethanol / 0.67 h / Ambient temperature

5: 99 percent / pyridine / 2 h / Ambient temperature

6: 99 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

7: 100 percent / 1N aq. HCl / acetone / 1.5 h / Ambient temperature

With pyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; nitric acid; nickel; sodium hydride; toluene-4-sulfonic acid; hydrazine hydrate; p-toluenesulfonyl chloride; lithium chloride; In tetrahydrofuran; diethyl ether; ethanol; acetone; benzene;
DOI:10.1016/S0040-4020(01)88513-6