[6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester

Base Information

Chemical Name:[6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester
CAS No.:108777-19-1
Molecular Formula:C₅₀H₇₈N₆O₈S
Molecular Weight:923.271
Hs Code.:

[6]6-benzyloxycarbonylamino-<i>lin</i>-penta[1=>6]hexanoylamino-hexanethioic acid <i>S</i>-phenyl ester

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Chemical Property of [6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester

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Technology Process of [6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester

There total 4 articles about [6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 108777-19-1
[6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

2: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

3: triethylamine; chlorocarbonic acid isobutyl ester; DMF / anschliessend Behandeln mit 6-Amino-hexansaeure und wss. NaOH

4: triethylamine; chlorocarbonic acid isobutyl ester; DMF / anschliessend Behandeln mit 6-<6-Amino-hexanoylamino>-hexanthiosaeure-S-phenylester-hydrobromid

With tetrahydrofuran; triethylamine; N,N-dimethyl-formamide; isobutyl chloroformate;

Reference yield:

: 49701-55-5
13-benzyloxycarbonylamino-8-oxo-7-azatridecanoic acid

: 108777-19-1
[6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

2: triethylamine; chlorocarbonic acid isobutyl ester; DMF / anschliessend Behandeln mit 6-Amino-hexansaeure und wss. NaOH

3: triethylamine; chlorocarbonic acid isobutyl ester; DMF / anschliessend Behandeln mit 6-<6-Amino-hexanoylamino>-hexanthiosaeure-S-phenylester-hydrobromid

With tetrahydrofuran; triethylamine; N,N-dimethyl-formamide; isobutyl chloroformate;

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 108777-19-1
[6]6-benzyloxycarbonylamino-lin-penta[1=>6]hexanoylamino-hexanethioic acid S-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: chlorocarbonic acid benzyl ester; aqueous NaOH

2: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

3: triethylamine; chlorocarbonic acid isobutyl ester; THF / Behandeln des erhaltenen Reaktionsgemisches mit 6-Amino-hexansaeure und wss. NaOH

4: triethylamine; chlorocarbonic acid isobutyl ester; DMF / anschliessend Behandeln mit 6-Amino-hexansaeure und wss. NaOH

5: triethylamine; chlorocarbonic acid isobutyl ester; DMF / anschliessend Behandeln mit 6-<6-Amino-hexanoylamino>-hexanthiosaeure-S-phenylester-hydrobromid

With tetrahydrofuran; sodium hydroxide; benzyl chloroformate; triethylamine; N,N-dimethyl-formamide; isobutyl chloroformate;