(Z)-5,9-dimethyl-4,8-decadiene-2-one diphenylmercaptal

Base Information

• Chemical Name: (Z)-5,9-dimethyl-4,8-decadiene-2-one diphenylmercaptal
• CAS No.: 114091-25-7
• Molecular Formula: C₂₄H₃₀S₂
• Molecular Weight: 382.634

Synonyms:

Chemical Property of (Z)-5,9-dimethyl-4,8-decadiene-2-one diphenylmercaptal

Chemical Property:

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Technology Process of (Z)-5,9-dimethyl-4,8-decadiene-2-one diphenylmercaptal

There total 1 articles about (Z)-5,9-dimethyl-4,8-decadiene-2-one diphenylmercaptal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nerol (106-25-2) → (Z)-5,9-dimethyl-4,8-decadiene-2-one diphenylmercaptal (114091-25-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) hexamethyl phosphoramide, triphenylmethane, methyllithium; 2) p-toluene sulfonyl chloride, LiCl / 1) ethyl ether, 0 deg C; 2) ethyl ether, 0 deg C, room temperature 15 h

2: 1) n-butyllithium / 1) THF, -20 deg C, 1 h; 2) -78 deg C then room temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; triphenylmethane; methyllithium; p-toluenesulfonyl chloride; lithium chloride;

DOI:10.1016/S0040-4020(01)86827-7

upstream raw materials:

Nerol

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