5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester

Base Information

Chemical Name:5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester
CAS No.:116928-17-7
Molecular Formula:C₃₂H₃₅CoO₆P₂S
Molecular Weight:668.633
Hs Code.:

5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester

Synonyms:

Suppliers and Price of 5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester

There total 1 articles about 5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 112792-44-6
dicarbonyl(η2-diethylthiophosphinito)(triphenylphosphane)cobalt(I)

: 603-35-0
triphenylphosphine

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 116928-17-7
5,5-dicarbonyl-2,2-diethyl-5-(triphenylphosphine)-1λ3-thia-2λ5-phospha-5-cobalta-1,3-cyclopentadiene-3,4-carboxylic acid diethyl ester

Guidance literature:: In toluene; To Co(CO)2PPh3SPEt2 and PPh3 was added EtO2CCCCO2Et dropwise at 55 °C. After 2 h the soln. was dried, CH3-Cy was added, filtered and dried, dissolved in EtOH/toluene, filtered. Soln. was dried, dissolved in toluene/EtOH for 24 h at -5 °C.; Crystn. at -30 °C, recrystn. from 15 ml toluene and 45 ml CH3-Cy at -5 °C after filtration, elem. anal.;