3-chloro-2,4,6-trimethoxy-toluene

Base Information

• Chemical Name: 3-chloro-2,4,6-trimethoxy-toluene
• CAS No.: 103323-77-9
• Molecular Formula: C₁₀H₁₃ClO₃
• Molecular Weight: 216.664
• Mol file: 103323-77-9.mol

Synonyms:

Chemical Property of 3-chloro-2,4,6-trimethoxy-toluene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-chloro-2,4,6-trimethoxy-toluene

There total 6 articles about 3-chloro-2,4,6-trimethoxy-toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-2,4,6-trimethoxybenzaldehyde (99070-86-7) → 3-chloro-2,4,6-trimethoxy-toluene (103323-77-9)

Guidance literature:

With hydrogenchloride; amalgamated zinc;

DOI:10.1039/jr9560003209

Reference yield:

1,2,3-trimethoxybenzene (621-23-8) → 3-chloro-2,4,6-trimethoxy-toluene (103323-77-9)

Guidance literature:

Multi-step reaction with 3 steps

1: CHCl₃; PCl₃

2: ZnCl₂; diethyl ether / beim Einleiten von HCl und Erhitzen des Reaktionsprodukts mit wss. NaOH

3: amalgamated zinc; aqueous HCl

With hydrogenchloride; amalgamated zinc; diethyl ether; chloroform; zinc(II) chloride; phosphorus trichloride;

DOI:10.1039/jr9560003209

Reference yield:

2,4,6-trimethoxychlorobenzene (67827-56-9) → 3-chloro-2,4,6-trimethoxy-toluene (103323-77-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ZnCl₂; diethyl ether / beim Einleiten von HCl und Erhitzen des Reaktionsprodukts mit wss. NaOH

2: amalgamated zinc; aqueous HCl

With hydrogenchloride; amalgamated zinc; diethyl ether; zinc(II) chloride;

DOI:10.1039/jr9560003209

upstream raw materials:

3-chloro-2,4,6-trimethoxybenzaldehyde

1,2,3-trimethoxybenzene

2,4,6-trimethoxychlorobenzene

(2,4,6-trimethoxy-phenyl)-acetic acid