ethyl 4--2-iodobutyrate

Base Information

• Chemical Name: ethyl 4--2-iodobutyrate
• CAS No.: 133719-39-8
• Molecular Formula: C₂₀H₂₈INO₆
• Molecular Weight: 505.35

Synonyms:

Chemical Property of ethyl 4--2-iodobutyrate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl 4--2-iodobutyrate

There total 2 articles about ethyl 4--2-iodobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-butyrate (133719-40-1) → ethyl 4--2-iodobutyrate (133719-39-8)

Guidance literature:

With iodine; lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 20 min;

DOI:10.1248/cpb.43.256

Reference yield:

→ ethyl 4--2-iodobutyrate (133719-39-8)

Guidance literature:

Reference yield:

ethyl 4--2-iodobutyrate (133719-39-8) + malononitrile (109-77-3) → ethyl 4--2-(dicyanomethyl)butyrate

Guidance literature:

With sodium hydride; dimethyl sulfoxide; Yield given. Multistep reaction; 1.) 0 deg C, 5 min, 2.) DMSO, RT, 1.5 h;

DOI:10.1248/cpb.43.256

upstream raw materials:

ethyl 4-butyrate

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