tetramethylammonium tris(thiobenzoato-O,S)tin(II)

Base Information

Chemical Name:tetramethylammonium tris(thiobenzoato-O,S)tin(II)
CAS No.:177413-19-3
Molecular Formula:C₄H₁₂N*C₂₁H₁₅O₃S₃Sn
Molecular Weight:604.402
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramethylammonium tris(thiobenzoato-O,S)tin(II)

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Technology Process of tetramethylammonium tris(thiobenzoato-O,S)tin(II)

There total 1 articles about tetramethylammonium tris(thiobenzoato-O,S)tin(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.7%

: 98-91-9
thiobenzoic acid

: 10025-69-1
tin(II) chloride dihdyrate

: 75-57-0
tetramethlyammonium chloride

: 121-44-8
triethylamine

: 177413-19-3
tetramethylammonium tris(thiobenzoato-O,S)tin(II)

Guidance literature:: In methanol; dichloromethane; acetonitrile; Ar-atmosphere; ratio SnCl2:Et3NH*SOCPh:Me4NCl=1:3:1, C7H6OH addn. to Et3N (MeOH), this soln. addn. to SnCl2 (MeOH) (pptn.), Me4NCl (MeOH) addn. with stirring, CH2Cl2 and MeCN addn., heating at 313 K for 30 min, filtering, stay to crystn. at 278 K; decantation, washing (MeOH, Et2O), drying (Ar-stream); elem. anal.;
DOI:10.1107/S0108270196000583