[Cd₂(N-(diisopropoxyphosphoryl)thiobenzamide-H)4]

Base Information

• Chemical Name: [Cd₂(N-(diisopropoxyphosphoryl)thiobenzamide-H)4]
• CAS No.: 923925-17-1
• Molecular Formula: C₅₂H₇₆Cd₂N₄O₁₂P₄S₄
• Molecular Weight: 1426.17
• Mol file: 923925-17-1.mol

Synonyms:

Chemical Property of [Cd₂(N-(diisopropoxyphosphoryl)thiobenzamide-H)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of [Cd₂(N-(diisopropoxyphosphoryl)thiobenzamide-H)4]

There total 1 articles about [Cd₂(N-(diisopropoxyphosphoryl)thiobenzamide-H)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

N-diisopropoxyphosphorylthiobenzamide (71039-21-9) + cadmium(II) acetate dihydrate (5743-04-4) + potassium hydroxide → [Cd(N-(diisopropoxyphosphorylthiobenzamide)2(N-(diisopropoxyphosphoryl)thiobenzamide-H)2] (923925-18-2) + [Cd2(N-(diisopropoxyphosphoryl)thiobenzamide-H)4] (923925-17-1)

Guidance literature:

In ethanol; water; suspn. of org. ligand (6 mmol) in aq. EtOH mixed with ethanolic soln. ofKOH (6 mmol); aq. soln. of Cd(CH3COO)2*2H2O (3 mmol) added dropwise (vi gorous stirring); stirred (room temp., 3 h); kept overnight; extd. with CH2Cl2; washed with water; dried over anhyd. MgSO4; solvent removed (vac.); extd. with n-hexane; residue recrystd. from CH2Cl2/n-hexane; second product isolated from hexane ext.; elem. anal.;

DOI:10.1002/ejic.200501005

upstream raw materials:

N-diisopropoxyphosphorylthiobenzamide

cadmium(II) acetate dihydrate