2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan

Base Information

Chemical Name:2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan
CAS No.:76707-25-0
Molecular Formula:C₃₀H₆₄F₂N₆Si₁₀
Molecular Weight:827.73
Hs Code.:

2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan

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Chemical Property of 2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan

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Technology Process of 2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan

There total 2 articles about 2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76707-21-6
1-Fluordimethylsilyl-3-(fluormethylphenyl)silyl-2.2.4.4.6.6-hexamethylcyclotrisilazan

: 76707-25-0
2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) RT, hexane; 2.) 12 h, reflux, THF;

Reference yield:

: 64639-32-3
1-(fluorodimethylsilyl)-2,2,4,4,6,6-hexamethylcyclotrisilazane

: 76707-25-0
2.2.4.4-Tetramethyl-1.3-bis<<2.2.4.4-tetramethyl-3-(fluormethylphenylsilyl-1.3-diaza-2.4-disilacyclobutyl)>dimethylsilyl>-1.3-diaza-2.4-disilacyclobutan

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-C₄H₉Li / 1.) RT, n-hexane; 2.) -60 deg C to RT

2: 1.) n-C₄H₉Li / 1.) RT, hexane; 2.) 12 h, reflux, THF

With n-butyllithium;