(9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-2,3,3a,5a,6,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalene-2-carboxylic acid methyl ester

Base Information

• Chemical Name: (9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-2,3,3a,5a,6,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalene-2-carboxylic acid methyl ester
• CAS No.: 128074-45-3
• Molecular Formula: C₂₆H₃₆O₅
• Molecular Weight: 428.569

Synonyms:

Chemical Property of (9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-2,3,3a,5a,6,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalene-2-carboxylic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-2,3,3a,5a,6,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalene-2-carboxylic acid methyl ester

There total 1 articles about (9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-2,3,3a,5a,6,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalene-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-((2E,8E,10E)-6-Benzyloxymethyl-12-chloro-2-methoxymethoxy-3-methyl-dodeca-2,8,10-trienyl)-malonic acid dimethyl ester (128094-58-6) → (9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-2,3,3a,5a,6,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalene-2-carboxylic acid methyl ester (128074-45-3) + (3aS,5aR,9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-1,3,3a,5a,6,7,8,9,9a,9b-decahydro-cyclopenta[a]naphthalene-2,2-dicarboxylic acid dimethyl ester + (3aR,5aS,9aS,9bS)-7-Benzyloxymethyl-9b-methoxymethoxy-9a-methyl-1,3,3a,5a,6,7,8,9,9a,9b-decahydro-cyclopenta[a]naphthalene-2,2-dicarboxylic acid dimethyl ester

Guidance literature:

With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 70 ℃; Yield given. Yields of byproduct given;

upstream raw materials:

2-((2E,8E,10E)-6-Benzyloxymethyl-12-chloro-2-methoxymethoxy-3-methyl-dodeca-2,8,10-trienyl)-malonic acid dimethyl ester

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