{Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆

Base Information

Chemical Name:{Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆
CAS No.:106252-53-3
Molecular Formula:C₄₇H₃₉N₂OOsP₂*F₆P
Molecular Weight:1052.89
Hs Code.:

{Os(C<sub>5</sub>D<sub>4</sub>N)2(P(C<sub>6</sub>H<sub>5</sub>)3)2(CO)H}<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>={Os(C<sub>5</sub>D<sub>4</sub>N)2(P(C<sub>6</sub>H<sub>5</sub>)3)2(CO)H}PF<sub>6</sub>

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Chemical Property of {Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆

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Technology Process of {Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆

There total 1 articles about {Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17084-13-8
potassium hexafluorophosphate

: 16971-31-6,36007-23-5
OsHCl(CO)(triphenylphosphine)₃

: 32190-42-4
2,2'-bipyridine-d8

: 106252-53-3
{Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆

Guidance literature:: In water; ethylene glycol; byproducts: PPh3, Cl(1-); refluxing equimolar amts. of the mer Os complex and the bipyridine in ethylene glycol (10 min), color change to yellow, cooling (room temp.), addn. of satd. aq. KPF6, pptn.; chromy. (alumina, 1:1 CH3CN/toluene), collection of the first yellow band, evapn., recrystn. from CH2Cl2 by slow addn. of ether;

Reference yield:

: 106252-53-3
{Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}⁽¹⁺⁾*PF₆^(1-)={Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H}PF₆

: 1493-13-6
trifluorormethanesulfonic acid

: 106252-56-6
{Os(C₅D₄N)2(P(C₆H₅)3)2(CO)H₂}⁽²⁺⁾

Guidance literature:: In dichloromethane; addn. of anhyd. trifluoromethanesulfonic acid to a soln. of the trans hydrido-Os complex in dry CF3COOH (room temp.) within an inert atmosphere drybox, color change from dark yellow to a pale clear yellow oil; not isolated; detn. by NMR;