{Co(S₂CN(CH₃)(C₆H₅))3}

Base Information

Chemical Name:{Co(S₂CN(CH₃)(C₆H₅))3}
CAS No.:86527-79-9
Molecular Formula:C₂₄H₂₄CoN₃S₆
Molecular Weight:605.864
Hs Code.:

{Co(S<sub>2</sub>CN(CH<sub>3</sub>)(C<sub>6</sub>H<sub>5</sub>))3}

Synonyms:

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Chemical Property of {Co(S₂CN(CH₃)(C₆H₅))3}

Chemical Property:

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Technology Process of {Co(S₂CN(CH₃)(C₆H₅))3}

There total 2 articles about {Co(S₂CN(CH₃)(C₆H₅))3} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cobalt(II) nitrate

: 39234-21-4
sodium N-methyl-N-phenyldithiocarbamate

: 86527-79-9
{Co(S₂CN(CH₃)(C₆H₅))3}

Guidance literature:: In water; solid Co salt adding to a soln. of freshly prepared Na dithiocarbamate in the presence of air, extg. via Soxhlet apparatus with CH2Cl2 or CHCl3, solvent removing;

Reference yield:

: carbonyl(η-5-cyclopentadienyl)diiodocobalt(III)

: 39234-21-4
sodium N-methyl-N-phenyldithiocarbamate

: 86527-79-9
{Co(S₂CN(CH₃)(C₆H₅))3}

: (C₅H₅)Co(S₂CN(CH₃)C₆H₅)I

Guidance literature:: In ethanol; dichloromethane; an ethanol soln. of Ph(Me)NCS2Na was added dropwise over a period of 20min to a soln. of CpCo(CO)I2 in CH2Cl2 at room temp. under N2, the mixt. was stirred for a further 20 min; the solvent was removed under reduced pressure, residue dissolved in CH2Cl2 and column chromd. on alumina, Co(S2CN(Me)Ph)3 being eluted with CH2Cl2 and CpCo(S2CN(Me)Ph)I - with 8:2 CH2Cl2/EtOH, the latter was crystd. from CH2Cl2/EtOH (elem. anal.);
DOI:10.1016/0022-328X(83)80110-7

Reference yield:

: 86527-79-9
{Co(S₂CN(CH₃)(C₆H₅))3}

: cobalt(II) bis(N-methyl-N-phenyl dithiocarbamate) monohydrate

: 62202-83-9
C₈H₈NS₂^(1-)

Guidance literature:: In dichloromethane; Electrochem. Process; cyclic voltammetry on Pt electrode at 22°C in CH2Cl2 in the presence of 0.1 M Bu4NClO4; electrochemical and spectrophotometrical monitoring;