trans-{Os(2,2'-bipyrazine)(PPh₃)2(CO)H}PF₆

Base Information

Chemical Name:trans-{Os(2,2'-bipyrazine)(PPh₃)2(CO)H}PF₆
CAS No.:89689-64-5
Molecular Formula:C₄₅H₃₇N₄OOsP₂*F₆P
Molecular Weight:1046.93
Hs Code.:

trans-{Os(2,2'-bipyrazine)(PPh<sub>3</sub>)2(CO)H}PF<sub>6</sub>

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Chemical Property of trans-{Os(2,2'-bipyrazine)(PPh₃)2(CO)H}PF₆

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Technology Process of trans-{Os(2,2'-bipyrazine)(PPh₃)2(CO)H}PF₆

There total 1 articles about trans-{Os(2,2'-bipyrazine)(PPh₃)2(CO)H}PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10199-00-5
2,2'-bipyrazine

: 36007-23-5
mer-Os(PPh₃)3(CO)HCl

: 89689-64-5
trans-{Os(2,2'-bipyrazine)(PPh₃)2(CO)H}PF₆

Guidance literature:: In ethylene glycol; byproducts: PPh3, Cl(1-); A soln. of complex in ethylene glycol was heated at reflux with a 5-fold excess of ligand for 20 min; cooled to room temp., aq. NH4PF6 was added;; ppt. was washed with H2O, ether, air-dried;;
DOI:10.1021/om00086a016