syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

Base Information

Chemical Name:syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate
CAS No.:103108-19-6
Molecular Formula:C₁₄H₂₀OS₂
Molecular Weight:268.444
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

Chemical Property:

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Technology Process of syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

There total 4 articles about syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22436-06-2,77943-96-5,78964-61-1,7384-80-7
2-methyl-3-phenylpropanol

: 103108-19-6,103108-20-9
anti-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Swern oxidation

2: 1.) n-butyllithium / 1.) hexane, THF, ether, -78 deg C, 15 min; 2.) hexane, THF, ether, -195 deg C, 30 min, from -195 deg C to -120 deg C, 30 min

With n-butyllithium;
DOI:10.1016/S0040-4020(01)96754-7

Reference yield:

: 22436-06-2,77943-96-5,78964-61-1,7384-80-7
2-methyl-3-phenylpropanol

: 103108-19-6,103108-20-9
syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Swern oxidation

2: 1.) n-butyllithium / 1.) hexane, THF, ether, -78 deg C, 15 min; 2.) hexane, THF, ether, -195 deg C, 30 min, from -195 deg C to -120 deg C, 30 min

With n-butyllithium;
DOI:10.1016/S0040-4020(01)96754-7

Reference yield:

: 870-73-5
ethyl dithioacetate

: 5445-77-2
2-benzylpropionaldehyde

: 103108-19-6,103108-20-9
anti-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

: 103108-19-6,103108-20-9
syn-ethyl 3-hydroxy-4-methyl-5-phenyldithiopentanoate

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) hexane, THF, ether, -78 deg C, 15 min; 2.) hexane, THF, ether, -120 deg C, 30 min;
DOI:10.1016/S0040-4020(01)96754-7