[CpFe(CO)2SeCO]2C₆H₃COCl

Base Information

• Chemical Name: [CpFe(CO)2SeCO]2C₆H₃COCl
• CAS No.: 1384426-24-7
• Molecular Formula: C₂₃H₁₃ClFe₂O₇Se₂
• Molecular Weight: 706.419

Synonyms:

Chemical Property of [CpFe(CO)2SeCO]2C₆H₃COCl

Chemical Property:

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Technology Process of [CpFe(CO)2SeCO]2C₆H₃COCl

There total 1 articles about [CpFe(CO)2SeCO]2C₆H₃COCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

((η5-C5H5)Fe(CO)2)2Se + 1,3,5-benzene tris(carbonyl chloride) (4422-95-1) → CpFe(CO)2SeCOC6H3(COCl)2 (1384426-18-9) + [CpFe(CO)2SeCO]2C6H3COCl (1384426-24-7)

Guidance literature:

In diethyl ether; under N2, Schlenk or vac. line technique; to Et2O soln. of Fe complex added dropwise at room temp. 1,3,5-C6H3(COCl)3 in Et2O; stirred for 4 h atroom temp.; volatiles removed in vac., residue redissolved in CH2Cl2, transferred into silica gel column; eluted with CH2Cl2/hexane (9:1 vol.); second band recrystd. from CH2Cl2/hexaneelem. anal.;

DOI:10.1002/zaac.201100541

upstream raw materials:

1,3,5-benzene tris(carbonyl chloride)

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