5,10,15-tris{2,6-bis(3,3-dimethylbutyryloxy)phenyl}-20-{2-{(3,5-bis(acetamido)benzoyloxy)}-6-(3,3-dimethylbutyryloxy)phenyl}porphinatoiron(III) bromide

Base Information

• Chemical Name: 5,10,15-tris{2,6-bis(3,3-dimethylbutyryloxy)phenyl}-20-{2-{(3,5-bis(acetamido)benzoyloxy)}-6-(3,3-dimethylbutyryloxy)phenyl}porphinatoiron(III) bromide
• CAS No.: 150953-58-5
• Molecular Formula: C₉₇H₁₀₈BrFeN₆O₁₈
• Molecular Weight: 1781.7

Synonyms:

Chemical Property of 5,10,15-tris{2,6-bis(3,3-dimethylbutyryloxy)phenyl}-20-{2-{(3,5-bis(acetamido)benzoyloxy)}-6-(3,3-dimethylbutyryloxy)phenyl}porphinatoiron(III) bromide

Chemical Property:

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Safty Information:

• Pictogram(s):  
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Technology Process of 5,10,15-tris{2,6-bis(3,3-dimethylbutyryloxy)phenyl}-20-{2-{(3,5-bis(acetamido)benzoyloxy)}-6-(3,3-dimethylbutyryloxy)phenyl}porphinatoiron(III) bromide

There total 1 articles about 5,10,15-tris{2,6-bis(3,3-dimethylbutyryloxy)phenyl}-20-{2-{(3,5-bis(acetamido)benzoyloxy)}-6-(3,3-dimethylbutyryloxy)phenyl}porphinatoiron(III) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,10,15-tris-(2,6-bis-(3,3-dimethylbutyryloxy)phenyl)-20-(2-((3,5-bis-(acetamido)benzoyloxy))-6-(3,3-dimethylbutyryloxy)phenyl)porphine + iron(II) bromide (7789-46-0) → 5,10,15-tris{2,6-bis(3,3-dimethylbutyryloxy)phenyl}-20-{2-{(3,5-bis(acetamido)benzoyloxy)}-6-(3,3-dimethylbutyryloxy)phenyl}porphinatoiron(III) bromide (150953-58-5)

Guidance literature:

In tetrahydrofuran; Ar atmosphere; refluxing (excess of FeBr2, 12 h); evapn. to dryness, extn. (CHCl3), chromy. (silica-gel column), treatment with aq. HBr, drying (room temp., vac., several hours);

DOI:10.1246/bcsj.66.1640

upstream raw materials:

iron(II) bromide

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