[Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n

Base Information

Chemical Name:[Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n
CAS No.:1037305-40-0
Molecular Formula:C₃H₇NO*C₈H₄O₄*Cd
Molecular Weight:349.622
Hs Code.:

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Chemical Property of [Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n

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Technology Process of [Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n

There total 2 articles about [Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: cadmium(II) nitrate tetrhydrate

: 100-21-0
terephthalic acid

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1037305-40-0
[Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n

Guidance literature:: In N,N-dimethyl-formamide; Cd-contg. compd. (1.69 mmol) and H2bdc (3.02 mmol) were added to DMF; stirring at 115°C until a colourless soln. was obtained; stirring was stopped, and the mixt. maintained at 115°C for a further 5 h; crystals were sepd. by filtration; elem. anal.;
DOI:10.1039/b718947h

Reference yield:

: cadmium(II) nitrate tetrhydrate

: 100-21-0
terephthalic acid

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1037305-40-0
[Cd(1,4-benzenedicarboxylate)(N,N-dimethylformamide)]n

: tetrakis(N,N-dimethylformamide)tris(1,4-benzenedicarboxylato)tricadmium

Guidance literature:: In N,N-dimethyl-formamide; Cd-contg. compd. (1.69 mmol) and H2bdc (3.02 mmol) were added to DMF; stirring at 95°C until a colourless soln. was obtained; stirring was stopped, and the mixt. maintained at 115°C for a further 5 h; crystals were sepd. by filtration; identified by powder XRD;
DOI:10.1039/b718947h