N-hippuroyl-DL-phenylalanine hydrazide

Base Information

• Chemical Name: N-hippuroyl-DL-phenylalanine hydrazide
• CAS No.: 98963-23-6
• Molecular Formula: C₁₈H₂₀N₄O₃
• Molecular Weight: 340.382
• Mol file: 98963-23-6.mol

Synonyms:

Chemical Property of N-hippuroyl-DL-phenylalanine hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-hippuroyl-DL-phenylalanine hydrazide

There total 5 articles about N-hippuroyl-DL-phenylalanine hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-Hippuroyl-N'-DL-phenylalanyl-hydrazin (99032-26-5) → N-hippuroyl-DL-phenylalanine hydrazide (98963-23-6)

Guidance literature:

With acetic acid; In 1,4-dioxane; at 40 ℃; Rate constant; other reaction partners, other solvents;

DOI:10.1002/hlca.19640470627

Reference yield:

N-hippuroyl-DL-phenylalanine ethyl ester (24629-17-2) → N-hippuroyl-DL-phenylalanine hydrazide (98963-23-6)

Guidance literature:

With ethanol; hydrazine hydrate;

Reference yield:

Phenylalanine (150-30-1,25191-15-5,658-69-5,67675-33-6) → N-hippuroyl-DL-phenylalanine hydrazide (98963-23-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / 60 - 70 °C

2: hydrochloric acid

3: absolute alcohol; hydrazine hydrate

With hydrogenchloride; sodium hydroxide; ethanol; hydrazine hydrate;

upstream raw materials:

N-hippuroyl-DL-phenylalanine ethyl ester

N-Hippuroyl-N'-DL-phenylalanyl-hydrazin

Phenylalanine

hippuroyl azide