11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 298220-46-9
• Molecular Formula: C₄₆H₆₈O₈S₂
• Molecular Weight: 813.173

Synonyms:

Chemical Property of 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

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Useful:

Technology Process of 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 3 articles about 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3α-hydroxy-11-oxo-cholanic acid (15173-31-6) → 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (298220-46-9)

Guidance literature:

Multi-step reaction with 2 steps

2: acetone

In acetone; 1: Acylation / 2: Substitution;

DOI:10.1016/S0040-4039(00)00886-8

Reference yield:

11-(α-bromophenylacetoxy)undecanoyl chloride → 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (298220-46-9)

Guidance literature:

Multi-step reaction with 2 steps

2: acetone

In acetone; 1: Acylation / 2: Substitution;

DOI:10.1016/S0040-4039(00)00886-8

Reference yield:

potassium ethyl xanthogenate (140-89-6) + 11-(2-Bromo-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester → 11-(2-Ethoxythiocarbonylsulfanyl-2-phenyl-acetoxy)-undecanoic acid (3R,5R,8S,9S,10S,13R,14S,17R)-17-((R)-3-carboxy-1-methyl-propyl)-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester (298220-46-9)

Guidance literature:

In acetone;

DOI:10.1016/S0040-4039(00)00886-8

upstream raw materials:

potassium ethyl xanthogenate

3α-hydroxy-11-oxo-cholanic acid

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