(N₃N)ReI

Base Information

• Chemical Name: (N₃N)ReI
• CAS No.: 881010-44-2
• Molecular Formula: C₂₅H₁₄F₁₅IN₄Re
• Molecular Weight: 968.501

Synonyms:

Chemical Property of (N₃N)ReI

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (N₃N)ReI

There total 2 articles about (N₃N)ReI which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

samarium diiodide (32248-43-4) + (HN3N)ReOCl → (N3N)ReI (881010-44-2)

Guidance literature:

In tetrahydrofuran; excess of SmI2 in 0.1 M THF soln. was added to Re-compd. soln. in THF atroom temp., under N2, stirring for 12 h; solvent was removed, toluene was added, soln. was filtered through Celite, storage at -25 °C, elem. anal.;

DOI:10.1002/zaac.200500088

Reference yield: 10.0%

samarium diiodide (32248-43-4) + (HN3N)ReOCl → (N3N)ReI (881010-44-2) + (HN3N)ReOI + (HN3N(*))ReF0.35I0.65

Guidance literature:

In tetrahydrofuran; 1 equiv. of SmI2 in 0.1 M THF soln. was added to Re-compd. soln. in THF at room temp., under N2, stirring for 1 h, soln. was filtered, exposed to air for 10 min; soln. was filtered, solvent was removed, toluene was added, soln. was filtered through Celite, storage at -25 °C, oxo-iodide was been able to sep., elem. anal.; C6F4-compd. was also isolated during separation experiments;

DOI:10.1002/zaac.200500088

upstream raw materials:

samarium diiodide

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