RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)⁽¹⁺⁾*C₁₈H₁₃O₈^(1-)=[RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)]C₁₈H₁₃O₈

Base Information

• Chemical Name: RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)⁽¹⁺⁾*C₁₈H₁₃O₈^(1-)=[RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)]C₁₈H₁₃O₈
• CAS No.: 97806-05-8
• Molecular Formula: C₁₈H₁₃O₈*C₄₈H₅₁NOP₃Ru
• Molecular Weight: 1209.23

Synonyms:

Chemical Property of RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)⁽¹⁺⁾*C₁₈H₁₃O₈^(1-)=[RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)]C₁₈H₁₃O₈

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Technology Process of RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)⁽¹⁺⁾*C₁₈H₁₃O₈^(1-)=[RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)]C₁₈H₁₃O₈

There total 1 articles about RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)⁽¹⁺⁾*C₁₈H₁₃O₈^(1-)=[RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)]C₁₈H₁₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

silver (R,R)-hydrogendibenzoyltartrate + RuCH3(CO)((CH3)3CNC)(C41H39P3)(1+)*I(1-)=[RuCH3(CO)((CH3)3CNC)(C41H39P3)]I (102261-63-2) → RuCH3(CO)((CH3)3CNC)(C41H39P3)(1+)*C18H13O8(1-)=[RuCH3(CO)((CH3)3CNC)(C41H39P3)]C18H13O8 (97806-05-8) + (+)-{RuCH3(CO)(CNC(CH3)3)(1,1,1-tris(diphenylphosphinomethyl)ethane)} (+)-dibenzoylhydrogentartrate

Guidance literature:

In ethanol; dichloromethane; byproducts: AgI; N2-atmosphere; stirring of complex and Ag salt in ethanol at 40°C for 0.5 h;; cooling; centrifugation (AgI); the supernatant was collected, concd., and cooled; the ppt. of the diastereomeric salts was recrystd. five timesfrom CH2Cl2/Et2O yielding the (+)-isomer of the cationic Ru complex; (-)-isomer in the mother liquors;;

DOI:10.1021/om00138a014

Reference yield:

RuCH3(CO)(P(CH3)2C6H5)(C41H39P3)(1+)*PF6(1-)=[RuCH3(CO)(P(CH3)2C6H5)(C41H39P3)]PF6 (102283-22-7) + RuCH3(CO)((CH3)3CNC)(C41H39P3)(1+)*C18H13O8(1-)=[RuCH3(CO)((CH3)3CNC)(C41H39P3)]C18H13O8 (97806-05-8) → {RuCH3(CO)(CNC(CH3)3)(1,1,1-tris(diphenylphosphinomethyl)ethane)} hexafluorophosphate

Guidance literature:

In chloroform-d1; N2 atmosphere; not isolated, detd. by NMR spectroscopy;

DOI:10.1021/om00138a014

upstream raw materials:

RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)⁽¹⁺⁾*I^(1-)=[RuCH₃(CO)((CH₃)3CNC)(C₄₁H₃₉P₃)]I

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