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1,4,8,11,15,18,22,25-octakis(decyl)phthalocyaninato zinc

Base Information
  • Chemical Name:1,4,8,11,15,18,22,25-octakis(decyl)phthalocyaninato zinc
  • CAS No.:138497-25-3
  • Molecular Formula:C112H176N8Zn
  • Molecular Weight:1700.07
  • Hs Code.:
1,4,8,11,15,18,22,25-octakis(decyl)phthalocyaninato zinc

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Chemical Property of 1,4,8,11,15,18,22,25-octakis(decyl)phthalocyaninato zinc
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Technology Process of 1,4,8,11,15,18,22,25-octakis(decyl)phthalocyaninato zinc

There total 2 articles about 1,4,8,11,15,18,22,25-octakis(decyl)phthalocyaninato zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In pentan-1-ol; under Ar atm. mixt. phthalonitriles, Zn(AcO)2*2H2O and 1,8-diazabicyclo(5.4.0)undec-7-ene in n-pentanol was refluxed for 12 h; mixt. was cooled to room temp., evapd. under vac., chromd. on silica column (hexane/CH2Cl2, 3:2), repeated chromy. on silica column (petroleum ether (bp 40-60°C)/THF, 10:1); elem. anal.;
DOI:10.1016/j.poly.2007.12.020
Guidance literature:
3,6-diphenylphthalatonitrile; 3,6-bis(decyl)phthalonitrile; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pentan-1-ol; for 1h; Inert atmosphere; Heating;
zinc(II) acetate dihydrate; In pentan-1-ol; for 20h; Inert atmosphere; Heating;
DOI:10.1142/S108842461330005X
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