[2,10,16,24-tetrakis(1a-hydronaphtho[b]-naphthofuro[3,2-d]-7,10-dyl-4-oxyphthalo-nitrile)-phthalocyaninatocobalt(II)]

Base Information

Chemical Name:[2,10,16,24-tetrakis(1a-hydronaphtho[b]-naphthofuro[3,2-d]-7,10-dyl-4-oxyphthalo-nitrile)-phthalocyaninatocobalt(II)]
CAS No.:952116-58-4
Molecular Formula:C₁₅₂H₇₂CoN₁₆O₁₆
Molecular Weight:2437.33
Hs Code.:

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Chemical Property of [2,10,16,24-tetrakis(1a-hydronaphtho[b]-naphthofuro[3,2-d]-7,10-dyl-4-oxyphthalo-nitrile)-phthalocyaninatocobalt(II)]

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Technology Process of [2,10,16,24-tetrakis(1a-hydronaphtho[b]-naphthofuro[3,2-d]-7,10-dyl-4-oxyphthalo-nitrile)-phthalocyaninatocobalt(II)]

There total 1 articles about [2,10,16,24-tetrakis(1a-hydronaphtho[b]-naphthofuro[3,2-d]-7,10-dyl-4-oxyphthalo-nitrile)-phthalocyaninatocobalt(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.5%

: 4,4'-(1a,8b-dihydronaphtho[b]naphthofuro[3,2-d]-furan-7,10-diyl)bis(oxy)diphthalonitrile

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 952116-58-4
[2,10,16,24-tetrakis(1a-hydronaphtho[b]-naphthofuro[3,2-d]-7,10-dyl-4-oxyphthalo-nitrile)-phthalocyaninatocobalt(II)]

: 952116-60-8
[1'a,8'b-tetrakis-bis[(2',10',16',24')-phthalocyaninatocobalt(II)]dioxynaphtho-[b]-naphthofuro[3,2-d]furan-7,10-diyl]

Guidance literature:: In neat (no solvent); (N2); mixture of diphthalonitrile-derivative and Co(OAc)2*4H2O powdered in a quartz crucible and heated in a sealed glass tube for 5 min under dry N2 at 280°C; cooling to room temp.; dissolved in DMF; precipitated by adding water; filtered, washed with hot water, hot ethanol, and dried in vacuo; product washed with acetic acid, methanol, ethanol, CH3CN and acetone for 12 h; chromy.(silica gel, CHCl3, CHCl3-THF gradient); elem. anal.;
DOI:10.1016/j.poly.2007.03.047