Benzaldehyde, 4-[(4-methylphenyl)thio]-

Base Information

• Chemical Name: Benzaldehyde, 4-[(4-methylphenyl)thio]-
• CAS No.: 141339-95-9
• Molecular Formula: C14H12OS
• Molecular Weight: 228.315
• Mol file: 141339-95-9.mol

Synonyms:

Chemical Property of Benzaldehyde, 4-[(4-methylphenyl)thio]-

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of Benzaldehyde, 4-[(4-methylphenyl)thio]-

There total 18 articles about Benzaldehyde, 4-[(4-methylphenyl)thio]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

para-thiocresol (106-45-6) + p-(iodophenyl)carboxaldehyde (15164-44-0) → 4-(p-tolyl)sulfanylbenzaldehyde (141339-95-9)

Guidance literature:

With 2,6-dimethylpyridine; In acetonitrile; at 20 ℃; for 48h; Catalytic behavior; Inert atmosphere; Irradiation;

DOI:10.1002/anie.201809493

Reference yield: 95.0%

di(p-tolyl) disulfide (103-19-5) + 4-bromo-benzaldehyde (1122-91-4) → 4-(p-tolyl)sulfanylbenzaldehyde (141339-95-9)

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; In water; N,N-dimethyl-formamide; at 80 ℃; for 5h;

DOI:10.1039/d0ra00719f

Reference yield: 95.0%

1-formaldehyde-4-(4-toluenesulfinyl)benzene → 4-(p-tolyl)sulfanylbenzaldehyde (141339-95-9)

Guidance literature:

With indium; molybdenum(V) chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

DOI:10.1080/00397910701544729

upstream raw materials:

(4-cyanophenyl)(4-methylphenyl)sulfide

di-(p-tolyl)sulfane

4-chlorobenzaldehyde

para-thiocresol

Downstream raw materials:

C₂₆H₂₁NOS₂

6-methyl-2-thioxo-4-(4-p-tolylsulfanyl-phenyl)-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

6-methyl-2-oxo-4-(4-p-tolylsulfanyl-phenyl)-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

1-[6-methyl-2-thioxo-4-(4-p-tolylsulfanyl-phenyl)-1,2,3,4-tetrahydro-pyrimidin-5-yl]-ethanone

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