2,5-bis{pyridyl-⁽²⁾-methylamino}-terephthalic acid diethylester

Base Information

• Chemical Name: 2,5-bis{pyridyl-⁽²⁾-methylamino}-terephthalic acid diethylester
• CAS No.: 102956-16-1
• Molecular Formula: C₂₄H₂₆N₄O₄
• Molecular Weight: 434.495
• Mol file: 102956-16-1.mol

Synonyms:

Chemical Property of 2,5-bis{pyridyl-⁽²⁾-methylamino}-terephthalic acid diethylester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,5-bis{pyridyl-⁽²⁾-methylamino}-terephthalic acid diethylester

There total 1 articles about 2,5-bis{pyridyl-⁽²⁾-methylamino}-terephthalic acid diethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-bis-[2]pyridylmethylimino-cyclohexane-1,4-dicarboxylic acid diethyl ester (103047-18-3) → 2,5-bis{pyridyl-(2)-methylamino}-terephthalic acid diethylester (102956-16-1)

Guidance literature:

With ethanol; iodine;

Reference yield:

cobalt(II) nitrate hexahydrate + 2,5-bis{pyridyl-(2)-methylamino}-terephthalic acid diethylester (102956-16-1) → cobalt(II) nitrate * 2.5-bis{pyridyl-(2)-methylamino}-terephthalic acid diethylester

Guidance literature:

In ethanol; formation from ester and Co(NO3)2*6H2O in alcohol at low temps.; pptn. at heating; sepn. after cooling down;; washing with alcohol; drying over silica gel; contains a small amount of solvent;;

Reference yield:

cobalt(II) chloride hexahydrate + 2,5-bis{pyridyl-(2)-methylamino}-terephthalic acid diethylester (102956-16-1) → 2 cobalt(II) chloride * 2.5-bis{pyridyl-(2)-methylamino}-terephthalic acid diethylester

Guidance literature:

In ethanol; formation from the alc. solns. of the ester and CoCl2*6H2O; heating the ppt.; after addn. of further CoCl2 crystals formed;; washing with alcohol;;

upstream raw materials:

2,5-bis-[2]pyridylmethylimino-cyclohexane-1,4-dicarboxylic acid diethyl ester

Downstream raw materials:

2,5-bis-([2]pyridylmethyl-amino)-terephthalic acid