24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone

Base Information

Chemical Name:24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone
CAS No.:122678-19-7
Molecular Formula:C₃₇H₄₅N₃O
Molecular Weight:547.784
Hs Code.:

Synonyms:

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Chemical Property of 24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone

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Technology Process of 24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone

There total 5 articles about 24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14956-27-5
5-chloro-3β-acetoxy-24.24-diphenyl-5α-cholene-(23)

: 122678-19-7
24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone

Guidance literature:: Multi-step reaction with 4 steps

1: tetrachloromethane; N-bromo-succinimide / Kochen unter der Einwirkung von Licht und anschliessend mit N_.N-Dimethyl-anilin

2: K₂CO₃

3: cyclohexanone; aluminium isopropylate; toluene

With tetrachloromethane; N-Bromosuccinimide; cyclohexanone; aluminum isopropoxide; potassium carbonate; toluene;
DOI:10.1002/hlca.19460290314

Reference yield:

: 108516-77-4
3β-acetoxy-24,24-diphenyl-chola-5,23-diene

: 122678-19-7
24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone

Guidance literature:: Multi-step reaction with 5 steps

1: chloroform; glacial acetic acid; HCl / 0 °C

2: tetrachloromethane; N-bromo-succinimide / Kochen unter der Einwirkung von Licht und anschliessend mit N_.N-Dimethyl-anilin

3: K₂CO₃

4: cyclohexanone; aluminium isopropylate; toluene

With hydrogenchloride; tetrachloromethane; N-Bromosuccinimide; chloroform; cyclohexanone; aluminum isopropoxide; potassium carbonate; acetic acid; toluene;
DOI:10.1002/hlca.19460290314

Reference yield:

: 108516-75-2
3β-acetoxy-24,24-diphenyl-chola-5,20(22)ξ,23-triene

: 122678-19-7
24,24-diphenyl-chola-4,20(22)ξ,23-trien-3-one semicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃

2: cyclohexanone; aluminium isopropylate; toluene

With cyclohexanone; aluminum isopropoxide; potassium carbonate; toluene;
DOI:10.1002/hlca.19460290314