[OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

Base Information

Chemical Name:[OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]
CAS No.:105059-08-3
Molecular Formula:C₁₉H₂₁ClF₆OP₂Pd
Molecular Weight:583.186
Hs Code.:

[OC(CF<sub>3</sub>)2CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2PdCl(P(CH<sub>3</sub>)3)]

Synonyms:

Suppliers and Price of [OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

Chemical Property:

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Technology Process of [OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

There total 2 articles about [OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105119-02-6,98331-70-5
[(OC(CF₃)2CH₂P(C₆H₅)2)2Pd]

: 105059-08-3
[OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

Guidance literature:: Multi-step reaction with 2 steps

1: acetone; chloroform

2: ethanol

In ethanol; chloroform; acetone;
DOI:10.1016/S0020-1693(00)82183-0

Reference yield:

: 19471-52-4
AgI*P(CH₃)3

: 105059-05-0
[(OC(CF₃)2CH₂P(C₆H₅)2PdCl)2]

: 105059-08-3
[OC(CF₃)2CH₂P(C₆H₅)2PdCl(P(CH₃)3)]

Guidance literature:: In ethanol; placing bridged complex and AgI(P(CH3)3) (20% excess) in separate arms of evacuated manifold; condensing dry C2H5OH onto the former; heating AgI(P(CH3)3) to about 240°C with cooling of the other arm to 77K; allowing soln. to warming to room temp.; removal of solvent (residue oil), taking up residue in the miniumum quantity of CH2Cl2; addn. of hexane; pptg.; washing ppt. with ether;;
DOI:10.1016/S0020-1693(00)82183-0