Mn(η5-C5H4Me)(CO)2((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

Base Information

Chemical Name:Mn(η5-C5H4Me)(CO)2((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)
CAS No.:915799-19-8
Molecular Formula:C₃₄H₃₄MnN₂O₂P
Molecular Weight:588.568
Hs Code.:

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Chemical Property of Mn(η5-C5H4Me)(CO)2((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

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Technology Process of Mn(η5-C5H4Me)(CO)2((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

There total 1 articles about Mn(η5-C5H4Me)(CO)2((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 915799-17-6
1,8-bis(dimethylamino)-2-(diphenylphosphanyl)-naphthalene

: methylcyclopentadienyl manganese(I) tricarbonyl

: 915799-19-8
Mn(η5-C5H4Me)(CO)2((1,8-bis(dimethylamino)naphthalen-2-yl)diphenylphosphine)

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); under N2; a THF degassed soln. of Mn-contg. compd. (0.98 mmol) was irradiated for 4 h with stirring at (-32) - (+40)°C; cooling to -78°C; degassed soln. of NMe2-contg. compd. (0.98 mmol) in THF was slowly added; stirring for 2.5 h; after stirring at 0°C overnight and at room temp. for 24 h, crystals were obtained by diffusion of pentane into a CH2Cl2 soln. of the complex;
DOI:10.1039/b609561e