trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate

Base Information

Chemical Name:trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate
CAS No.:835890-11-4
Molecular Formula:C₆₄H₅₆IrO₃P₂*F₆Sb
Molecular Weight:1365.04
Hs Code.:

trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate

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Chemical Property of trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate

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Technology Process of trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate

There total 1 articles about trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 515160-93-7
trans-[IrH(PPh₃)2(C(C₆H₅)=CHC(CH₃)O)(acetone)]SbF₆

: 54159-16-9
(2-<2H1>)-4-methoxyphenylethyne

: 835890-11-4
trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(1,4-di-p-methoxyphenylbuta-1,4-dien-2-yl)iridium(III) hexafluoroantimonate

Guidance literature:: In dichloromethane; (Ar); alkyne (2 equiv.) was added via syringe to stirred soln. of Ir complex in CH2Cl2; soln. was stirred at room temp. for 2 h; concd. (vac.); Et2O added; washed (Et2O); filtered; dried (vac.);
DOI:10.1021/om049271z