(4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

Base Information

• Chemical Name: (4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester
• CAS No.: 86318-89-0
• Molecular Formula: C₅₅H₅₂ClN₆O₁₁P
• Molecular Weight: 1039.48

Synonyms:

Chemical Property of (4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

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Technology Process of (4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

There total 1 articles about (4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5'-O-(4,4'-dimethoxytrityl)-2'-O-tetrahydrofuran-2-yl-N6-benzoyl-D-adenosine (86318-86-7) + o-chlorophenyl phosphoro-p-anisidochloridate (82556-11-4) → (4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester (86318-89-0)

Guidance literature:

Reference yield:

(4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester (86318-89-0) → (4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester (86318-93-6)

Guidance literature:

With zinc dibromide;

upstream raw materials:

5'-O-(4,4'-dimethoxytrityl)-2'-O-tetrahydrofuran-2-yl-N⁶-benzoyl-D-adenosine

o-chlorophenyl phosphoro-p-anisidochloridate

Downstream raw materials:

(4-Methoxy-phenyl)-phosphoramidic acid (2R,3R,4R,5R)-5-(6-benzoylamino-purin-9-yl)-2-hydroxymethyl-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester

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