<(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester

Base Information

• Chemical Name: <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester
• CAS No.: 139512-52-0
• Molecular Formula: C₅₂H₅₉N₃O₁₁S
• Molecular Weight: 935.112

Synonyms:

Chemical Property of <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester

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Technology Process of <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester

There total 2 articles about <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<(N-p-methoxybenzyloxycarbonyl)-α-p-methoxybenzyl-δ-((R)-α-aminoadipoyl)>-S-p-methoxybenzyl-L-cysteine (163192-65-2) + D/L-(2-2H)-valine benzhydryl ester tosyl ammonium salt → <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-D-(2-2H)-valine benzhydryl ester (139512-52-0) + <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester (139512-52-0)

Guidance literature:

With sodium hydrogencarbonate; sodium sulfate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; Yield given. Multistep reaction; 2) CH₂Cl₂, RT, 24h;

DOI:10.1016/S0040-4020(01)80725-0

Reference yield:

<(N-p-methoxybenzyloxycarbonyl)-α-p-methoxybenzyl-δ-((R)-α-aminoadipoyl)>-S-p-methoxybenzyl-L-cysteine (163192-65-2) + D/L-(2-2H)-valine benzhydryl ester tosyl ammonium salt → <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-D-(2-2H)-valine benzhydryl ester (139512-52-0) + <(5R)-5-N-p-methoxybenzyloxycarbonylamino-5-p-methoxybenzylcarbonylpentanamido>-S-p-methoxybenzyl-L-cysteinyl-L-(2-2H)-valine benzhydryl ester (139512-52-0)

Guidance literature:

With sodium hydrogencarbonate; sodium sulfate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; Yield given. Multistep reaction; 2) CH₂Cl₂, RT, 24h;

DOI:10.1016/S0040-4020(01)80725-0

upstream raw materials:

<(N-p-methoxybenzyloxycarbonyl)-α-p-methoxybenzyl-δ-((R)-α-aminoadipoyl)>-S-p-methoxybenzyl-L-cysteine

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