hexamethyl-1,5-bistrisiloxane

Base Information

Chemical Name:hexamethyl-1,5-bistrisiloxane
CAS No.:107394-34-3
Molecular Formula:C₄₂H₄₆O₂P₂Si₃
Molecular Weight:729.03
Hs Code.:

hexamethyl-1,5-bis<p-(diphenylphosphino)phenyl>trisiloxane

Synonyms:

Suppliers and Price of hexamethyl-1,5-bistrisiloxane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hexamethyl-1,5-bistrisiloxane

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Technology Process of hexamethyl-1,5-bistrisiloxane

There total 1 articles about hexamethyl-1,5-bistrisiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3582-71-6
1,5-dichlorohexamethyltrisiloxane

: 734-59-8
(4-bromophenyl)diphenylphosphane

: 107394-34-3
hexamethyl-1,5-bistrisiloxane

Guidance literature:: With n-butyllithium; water; Yield given. Multistep reaction; 1.) diethyl ether, hexane, -70 deg C -> r.t., 2,5 h; 2.) r.t., overnight;
DOI:10.1016/0022-328X(89)80021-X

Reference yield: 41.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 107394-34-3
hexamethyl-1,5-bistrisiloxane

: 148573-90-4
PdCl₂(((C₆H₅)2PC₆H₄Si(CH₃)2OSi(CH₃)2OSi(CH₃)2C₆H₄P(C₆H₅)2))

Guidance literature:: In benzene; stirring (room temp., 24 h), pptn. (according to W. L. Steffen and G. J. Palenik, Inorg. Chem., 15 (1976) 2432); filtration, washing (benzene), drying (vac.);
DOI:10.1016/0304-5102(93)85084-7