Moluccanin

Base Information

• Chemical Name: Moluccanin
• CAS No.: 116521-73-4
• Molecular Formula: C₂₀H₁₈O₈
• Molecular Weight: 386.358
• Mol file: 116521-73-4.mol

Synonyms:Moluccanin

Chemical Property of Moluccanin

Chemical Property:

• Boiling Point: 619.1±55.0 °C(Predicted)
• PKA: 9.70±0.40(Predicted)
• PSA: 107.59000
• Density: 1.403±0.06 g/cm3(Predicted)
• LogP: 2.38920

Purity/Quality:

≥98% ^*data from raw suppliers

Moluccanin ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Moluccanin

There total 5 articles about Moluccanin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 7.1%

aesculetin (305-01-1) + trans-sinapyl alcohol (20675-96-1) → (2S,3S)-2-(4-Hydroxy-3,5-dimethoxy-phenyl)-3-hydroxymethyl-2,3-dihydro-1,4,5-trioxa-anthracen-6-one + molucannin (116521-73-4)

Guidance literature:

With silver(l) oxide; In methanol; benzene; for 48h; Ambient temperature;

Reference yield:

trans-3,5-dimethoxy-4-hydroxycinnamic acid (530-59-6,7362-37-0) → molucannin (116521-73-4)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine / 3 h / 100 °C

2: diethyl ether / Ambient temperature

3: LiAlH₄

4: 7.1 percent / Ag₂O / benzene; methanol / 48 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; silver(l) oxide; In methanol; diethyl ether; benzene;

Reference yield:

esculin (531-75-9,97882-87-6) → molucannin (116521-73-4)

Guidance literature:

Multi-step reaction with 2 steps

1: β-glucosidase, acetate buffer (pH 5.0) / 37 °C

2: 7.1 percent / Ag₂O / benzene; methanol / 48 h / Ambient temperature

With acetate buffer; silver(l) oxide; β-glucosidase; In methanol; benzene;

upstream raw materials:

aesculetin

trans-sinapyl alcohol

trans-3,5-dimethoxy-4-hydroxycinnamic acid

(E)-4-acetoxy-3,5-dimethoxycinnamic acid

Refernces