lithium tetrahydroborate * 3 p-benzylpyridine

Base Information

• Chemical Name: lithium tetrahydroborate * 3 p-benzylpyridine
• CAS No.: 244761-19-1
• Molecular Formula: C₃₆H₃₇BLiN₃
• Molecular Weight: 529.462
• Mol file: 244761-19-1.mol

Synonyms:

Chemical Property of lithium tetrahydroborate * 3 p-benzylpyridine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of lithium tetrahydroborate * 3 p-benzylpyridine

There total 1 articles about lithium tetrahydroborate * 3 p-benzylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

lithium borohydride + 4-benzyl pyridine (2116-65-6) → lithium tetrahydroborate * 3 p-benzylpyridine (244761-19-1)

Guidance literature:

In toluene; N2-atmosphere; excess benzylpyridine, stirring for 2 d; filtration, crystn. (8°C, 5 d); elem. anal.;

DOI:10.1021/ic990205c

Reference yield:

lithium tetrahydroborate * 3 p-benzylpyridine (244761-19-1) → H3B * p-benzylpyridine

Guidance literature:

In benzene-d6; N2-atmosphere; dissoln. in C6D6/p-benzylpyridine=4:1; not isolated, detd. by (11)B-NMR spectroscopy;

DOI:10.1021/ic990205c

upstream raw materials:

4-benzyl pyridine