Br₂Pd(C₆H₃(CH(CH₃)2)2NCClCClNC₆H₃(CH(CH₃)2)2)

Base Information

• Chemical Name: Br₂Pd(C₆H₃(CH(CH₃)2)2NCClCClNC₆H₃(CH(CH₃)2)2)
• CAS No.: 1227479-98-2
• Molecular Formula: C₂₆H₃₄Br₂Cl₂N₂Pd
• Molecular Weight: 711.703
• Mol file: 1227479-98-2.mol

Synonyms:

Chemical Property of Br₂Pd(C₆H₃(CH(CH₃)2)2NCClCClNC₆H₃(CH(CH₃)2)2)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Br₂Pd(C₆H₃(CH(CH₃)2)2NCClCClNC₆H₃(CH(CH₃)2)2)

There total 1 articles about Br₂Pd(C₆H₃(CH(CH₃)2)2NCClCClNC₆H₃(CH(CH₃)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.1%

N,N-Bis-<2,6-Diisopropylphenyl>-oxalimidoylchlorid (167966-57-6) + palladium(II) bromide (13444-94-5) → Br2Pd(C6H3(CH(CH3)2)2NCClCClNC6H3(CH(CH3)2)2) (1227479-98-2)

Guidance literature:

In tetrahydrofuran; cooled (-78°C) soln. of Me2C6H3NC(Cl)C(Cl)NC6H3Me2 in THF added soln. of PdBr2 in THF; react. mixt. stirred for 18 h; temp. raised to ro om temp; filtered; volatiles removed; washed with pentane, then with Et2O; filtered, dried under reduced pressure overnight; elem. anal.;

DOI:10.1016/j.ica.2009.11.009

upstream raw materials:

N,N-Bis-<2,6-Diisopropylphenyl>-oxalimidoylchlorid

palladium(II) bromide