ent-6β,21;6'β,21'-diepoxy-2'-hydroxy-17'-(4-iodo-benzoyloxy)-2,3-didehydro-(7βC⁴'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester

Base Information

• Chemical Name: ent-6β,21;6'β,21'-diepoxy-2'-hydroxy-17'-(4-iodo-benzoyloxy)-2,3-didehydro-(7βC⁴'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester
• CAS No.: 38741-20-7
• Molecular Formula: C₄₉H₅₁IN₄O₇
• Molecular Weight: 934.871
• Mol file: 38741-20-7.mol

Synonyms:

Chemical Property of ent-6β,21;6'β,21'-diepoxy-2'-hydroxy-17'-(4-iodo-benzoyloxy)-2,3-didehydro-(7βC⁴'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ent-6β,21;6'β,21'-diepoxy-2'-hydroxy-17'-(4-iodo-benzoyloxy)-2,3-didehydro-(7βC⁴'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester

There total 1 articles about ent-6β,21;6'β,21'-diepoxy-2'-hydroxy-17'-(4-iodo-benzoyloxy)-2,3-didehydro-(7βC⁴'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ent-6β,21;6'β,21'-diepoxy-2',17'-dihydroxy-2,3-didehydro-(7βC4'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester (38790-81-7) + 4-iodobenzoic acid chloride (1711-02-0) → ent-6β,21;6'β,21'-diepoxy-2'-hydroxy-17'-(4-iodo-benzoyloxy)-2,3-didehydro-(7βC4'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester (38741-20-7)

Guidance literature:

With pyridine;

DOI:10.1002/hlca.19720550602

upstream raw materials:

ent-6β,21;6'β,21'-diepoxy-2',17'-dihydroxy-2,3-didehydro-(7βC^4'',3'β)-3',4''-dihydro-2'H-spiro[aspidospermidine-7,5''-pyrido[1',2',3':1,2,3]aspidospermidine]-3-carboxylic acid methyl ester

4-iodobenzoic acid chloride