Fe(meso-(4-F₃CPh)4octaethylporphyrinato)Cl

Base Information

• Chemical Name: Fe(meso-(4-F₃CPh)4octaethylporphyrinato)Cl
• CAS No.: 953387-03-6
• Molecular Formula: C₆₄H₅₆ClF₁₂FeN₄
• Molecular Weight: 1200.46

Synonyms:

Chemical Property of Fe(meso-(4-F₃CPh)4octaethylporphyrinato)Cl

Chemical Property:

Purity/Quality:

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Technology Process of Fe(meso-(4-F₃CPh)4octaethylporphyrinato)Cl

There total 1 articles about Fe(meso-(4-F₃CPh)4octaethylporphyrinato)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iron(II) chloride tetrahydrate + meso-(4-CF3Ph)4octaethylporphyrin → Fe(meso-(4-F3CPh)4octaethylporphyrinato)Cl (953387-03-6)

Guidance literature:

In methanol; chloroform; refluxing iron compd. and porphyrin deriv. in 3:1 mixt. of chloroform and methanol under Ar; treating with diluted aq. HCl, separating organic layer, drying over Na2SO4, evapn., chromy. (silica gel, CH2Cl2/CH3OH), (1)H NMR;

DOI:10.1021/ic700827w

Reference yield:

1H-imidazole (288-32-4) + Fe(meso-(4-F3CPh)4octaethylporphyrinato)Cl (953387-03-6) → [Fe(meso-(4-CF3-Ph)4octaethylporphyrinato)(imidazol)2]Cl (953386-82-8)

Guidance literature:

In dichloromethane; addn. of 6-10 equiv. of imidazol to CH2Cl2 soln. of iron compd. in NMR tube; not isolated, ESR;

DOI:10.1021/ic700827w

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + Fe(meso-(4-F3CPh)4octaethylporphyrinato)Cl (953387-03-6) + silver perchlorate → [Fe(meso-(4-CF3-Ph)4octaethylporphyrinato)(THF)2](perchlorate) (953387-24-1)

Guidance literature:

In tetrahydrofuran; addn. of silver compd. to soln. of iron compd. in THF;

DOI:10.1021/ic700827w

Downstream raw materials:

[Fe(meso-(4-CF₃-Ph)4octaethylporphyrinato)(imidazol)2]Cl

[Fe(meso-(4-CF₃-Ph)4octaethylporphyrinato)(THF)2](perchlorate)

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