CpRu(CO)(PMe₃)(PPh₂*BH₃)

Base Information

• Chemical Name: CpRu(CO)(PMe₃)(PPh₂*BH₃)
• CAS No.: 1036029-96-5
• Molecular Formula: C₂₁H₂₇BOP₂Ru
• Molecular Weight: 469.273
• Mol file: 1036029-96-5.mol

Synonyms:

Chemical Property of CpRu(CO)(PMe₃)(PPh₂*BH₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of CpRu(CO)(PMe₃)(PPh₂*BH₃)

There total 1 articles about CpRu(CO)(PMe₃)(PPh₂*BH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

CpRu(CO)2(PPh2*BH3) (1036029-95-4) + trimethylphosphane (594-09-2) → CpRu(CO)(PMe3)(PPh2*BH3) (1036029-96-5)

Guidance literature:

In tetrahydrofuran; under Ar; to a soln. of Ru-contg. compd. (0.261 mmol) in THF PMe3 (0.52 mmol) was added; stirring at 20°C; (11)B- and (14)P NMR spectra monitoring; after 3 d, the volatile compds.of the react. mixt. were removed in vac. overnight; the compd. was wash ed by filtration through celite supported on glass wool with Et2O-THF (5:1); storing at -40°C for 2 d;

DOI:10.1039/b718918d

upstream raw materials:

CpRu(CO)2(PPh₂*BH₃)

trimethylphosphane