(C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)][B(C₆H₃(CF₃)2)4]

Base Information

• Chemical Name: (C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)][B(C₆H₃(CF₃)2)4]
• CAS No.: 168283-48-5
• Molecular Formula: C₁₈H₃₆FeOPSi*C₃₂H₁₂BF₂₄
• Molecular Weight: 1246.61
• Mol file: 168283-48-5.mol

Synonyms:

Chemical Property of (C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)][B(C₆H₃(CF₃)2)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)][B(C₆H₃(CF₃)2)4]

There total 2 articles about (C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)⁽¹⁺⁾*B(C₆H₃(CF₃)2)4^(1-)=[(C₅H₅)Fe(CO)(P(C₂H₅)3)(HSi(C₂H₅)3)][B(C₆H₃(CF₃)2)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex + triethylsilane (617-86-7) + (C5H5)Fe(CO)(P(C2H5)3)(Si(C2H5)3) (168283-67-8) → (C5H5)Fe(CO)(P(C2H5)3)(HSi(C2H5)3)(1+)*B(C6H3(CF3)2)4(1-)=[(C5H5)Fe(CO)(P(C2H5)3)(HSi(C2H5)3)][B(C6H3(CF3)2)4] (168283-48-5)

Guidance literature:

In dichloromethane-d2; byproducts: H2; N2-atmosphere, NMR tube, -78°C;

Reference yield:

triethylsilane (617-86-7) + Brookhart's acid + (C5H5)Fe(CO)(P(C2H5)3)(Si(C2H5)3) (168283-67-8) → (C5H5)Fe(CO)(P(C2H5)3)(HSi(C2H5)3)(1+)*B(C6H3(CF3)2)4(1-)=[(C5H5)Fe(CO)(P(C2H5)3)(HSi(C2H5)3)][B(C6H3(CF3)2)4] (168283-48-5)

Guidance literature:

In dichloromethane-d2; byproducts: H2; N2-atmosphere; mixing equimolar amts. of Fe-complex and B-compd. at -78°C, addn. of 5 equiv. silane; not isolated, detd. by NMR spectroscopy;

DOI:10.1016/0022-328X(95)00117-9

upstream raw materials:

triethylsilane

(C₅H₅)Fe(CO)(P(C₂H₅)3)(Si(C₂H₅)3)