(4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine

Base Information

• Chemical Name: (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine
• CAS No.: 6068-48-0
• Molecular Formula: C₁₄H₁₅N₃O
• Molecular Weight: 241.293
• Mol file: 6068-48-0.mol

Synonyms:

Chemical Property of (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine

There total 5 articles about (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methyl-2,6-dimethylpyridin-4-one (767-83-9) → (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine (6068-48-0)

Guidance literature:

Multi-step reaction with 3 steps

1: benzenesulfonyl chloride; benzene / und Behandeln des erhaltenen Salzes mit Benzoesaeure-hydrazid in Aethanol

2: hydrochloric acid

3: sodium perchlorate; water / und Behandeln einer Loesung des erhaltenen Perchlorats in Ameisensaeure mit wss.Natronlauge

With hydrogenchloride; sodium perchlorate; water; benzenesulfonyl chloride; benzene;

Reference yield:

Dehydracetic acid (520-45-6,53488-80-5) → (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine (6068-48-0)

Guidance literature:

Multi-step reaction with 4 steps

1: water / 100 - 110 °C / unter Druck

2: benzenesulfonyl chloride; benzene / und Behandeln des erhaltenen Salzes mit Benzoesaeure-hydrazid in Aethanol

3: hydrochloric acid

4: sodium perchlorate; water / und Behandeln einer Loesung des erhaltenen Perchlorats in Ameisensaeure mit wss.Natronlauge

With hydrogenchloride; sodium perchlorate; water; benzenesulfonyl chloride; benzene;

Reference yield:

benzoic acid-(1,2,6-trimethyl-1H-[4]pyridylidenehydrazide) (100973-44-2) → (4-oxo-cyclohexa-2,5-dienylidene)-(1,2,6-trimethyl-1H-[4]pyridylidene)-hydrazine (6068-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrochloric acid

2: sodium perchlorate; water / und Behandeln einer Loesung des erhaltenen Perchlorats in Ameisensaeure mit wss.Natronlauge

With hydrogenchloride; sodium perchlorate; water;

upstream raw materials:

1,2,6-trimethyl-1H-pyridin-4-one-hydrazone; dihydrochloride

p-benzoquinone

N-methyl-2,6-dimethylpyridin-4-one

benzoic acid-(1,2,6-trimethyl-1H-[4]pyridylidenehydrazide)