CoBr₂(Ph-DAB)2

Base Information

• Chemical Name: CoBr₂(Ph-DAB)2
• CAS No.: 88177-85-9
• Molecular Formula: C₂₈H₂₄Br₂CoN₄
• Molecular Weight: 635.327

Synonyms:

Chemical Property of CoBr₂(Ph-DAB)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of CoBr₂(Ph-DAB)2

There total 2 articles about CoBr₂(Ph-DAB)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dibromo-bis-triphenylphosphine cobalt (14126-32-0) + 1,4-diphenyl-1,4-diaza-1,3-butadiene → CoBr2(Ph-DAB)2 (88177-85-9)

Guidance literature:

In acetone; Co-compd. in acetone was treated with an org. compd. (molar ratio Co:L = 1:1 - 1:2) under N2; stirring for 2 h at room temp.;; after filtration of the soln. the solvent was removed, leaving a purple oil; treatment of this oil with Et2O gave a purple solid, which was filtered off, washed with Et2O and dried in vacuo; elem. anal.;

DOI:10.1016/S0020-1693(00)81413-9

Reference yield:

1,4-diphenyl-1,4-diaza-1,3-butadiene + cobalt(II) bromide → CoBr2(Ph-DAB)2 (88177-85-9)

Guidance literature:

In acetone; Co-compd. in acetone was treated with an org. compd. (molar ratio Co:L = 1:1 - 1:2) under N2; stirring for 2 h at room temp.;; after filtration of the soln. the solvent was removed, leaving a purple oil; treatment of this oil with Et2O gave a purple solid, which was filtered off, washed with Et2O and dried in vacuo; elem. anal.;

DOI:10.1016/S0020-1693(00)81413-9

upstream raw materials:

dibromo-bis-triphenylphosphine cobalt

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