Co⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Co((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆

Base Information

• Chemical Name: Co⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Co((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆
• CAS No.: 578737-65-2
• Molecular Formula: C₂₄H₃₆N₄*Co*F₆P*NO₃
• Molecular Weight: 646.539

Synonyms:

Chemical Property of Co⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Co((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆

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Technology Process of Co⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Co((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆

There total 1 articles about Co⁽²⁺⁾*(C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2*NO₃^(1-)*PF₆^(1-)=[Co((C₃H₆)2(C₂H₄)2N₄H₂(CH₂C₆H₅)2)(NO₃)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

ammonium hexafluorophosphate + cobalt(II) nitrate hexahydrate + 1,11-dibenzyl-1,4,8,11-tetraazacyclotetradecane (151367-38-3) → Co(2+)*(C3H6)2(C2H4)2N4H2(CH2C6H5)2*NO3(1-)*PF6(1-)=[Co((C3H6)2(C2H4)2N4H2(CH2C6H5)2)(NO3)]PF6 (578737-65-2)

Guidance literature:

In methanol; Co-contg. compd. (0.132 mmol) in MeOH was added to a soln. of a ligand (0.132 mmol) in the same solvent; the soln. was refluxed for 1 h under N2and cooled to room temp.; the vol. of the soln. was reduced to 1/3 and excess satd. NH4PF6 in MeOH was added; dropwise addn. of ether; recrystn. from a mixt. of acetone, methanol andether; elem. anal.;

DOI:10.1039/b300002h

upstream raw materials:

1,11-dibenzyl-1,4,8,11-tetraazacyclotetradecane

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