O,O-Diethyl-S-β-styryl-phosphor-dithioester

Base Information

• Chemical Name: O,O-Diethyl-S-β-styryl-phosphor-dithioester
• CAS No.: 77392-39-3
• Molecular Formula: C₁₂H₁₇O₂PS₂
• Molecular Weight: 288.372
• Mol file: 77392-39-3.mol

Synonyms:

Chemical Property of O,O-Diethyl-S-β-styryl-phosphor-dithioester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O,O-Diethyl-S-β-styryl-phosphor-dithioester

There total 2 articles about O,O-Diethyl-S-β-styryl-phosphor-dithioester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(diethoxyphosphoryl)disulphide (2901-90-8) + β-styrylmagnesium bromide (30094-01-0,35672-47-0,56516-81-5) → O,O-Diethyl-S-β-styryl-phosphor-dithioester (77392-39-3)

Guidance literature:

In tetrahydrofuran; diethyl ether;

DOI:10.1016/S0040-4020(01)98479-0

Reference yield:

→ O,O-Diethyl-S-β-styryl-phosphor-dithioester (77392-39-3)

Guidance literature:

Bis-diethoxyphosphinothioyl-disulfid, Styryl-Mg-Br/Ae.;

DOI:10.1021/ja01508a064

upstream raw materials:

bis(diethoxyphosphoryl)disulphide

β-styrylmagnesium bromide