benzoyle-phenyle-azo-pyridinium-methylure

Base Information

• Chemical Name: benzoyle-phenyle-azo-pyridinium-methylure
• CAS No.: 59349-26-7
• Molecular Formula: C₁₉H₁₅N₃O
• Molecular Weight: 301.348
• Mol file: 59349-26-7.mol

Synonyms:

Chemical Property of benzoyle-phenyle-azo-pyridinium-methylure

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzoyle-phenyle-azo-pyridinium-methylure

There total 5 articles about benzoyle-phenyle-azo-pyridinium-methylure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,N'-diphenyl-glyoxylohydrazonoyl)-pyridinium; bromide → benzoyle-phenyle-azo-pyridinium-methylure (59349-26-7)

Guidance literature:

With sodium methylate;

Reference yield:

N-phenacylpyridinium bromide (16883-69-5) + aniline (62-53-3) → benzoyle-phenyle-azo-pyridinium-methylure (59349-26-7)

Guidance literature:

With hydrogenchloride; carbonate de soude; sodium nitrite; Multistep reaction; 1.) water, 0 deg C, 2.) pH= 8.0 - 8.5, water, 3 h;

DOI:10.1016/S0040-4020(01)91386-9

Reference yield:

N-phenacylpyridinium bromide (16883-69-5) → benzoyle-phenyle-azo-pyridinium-methylure (59349-26-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium acetate

2: aqueous sodium acetate solution

With sodium acetate;

upstream raw materials:

N-phenacylpyridinium bromide

aniline

Downstream raw materials:

3,6-Dibenzoyl-1,4-dihydro-1,4-diphenyl-1,2,4,5-tetrazine

3,6-dibenzoyl-1,4-dihydro-1,4-bis-(p-nitrophenyl)-1,2,4,5-tetrazine