(3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Base Information

Chemical Name:(3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol
CAS No.:136203-70-8
Molecular Formula:C₃₅H₅₄O₂
Molecular Weight:506.813
Hs Code.:

(3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

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Chemical Property of (3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

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Technology Process of (3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

There total 3 articles about (3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136203-68-4
(3S,5S,10S,13R,14R,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-3-hydroxy-10,13-dimethyl-1,2,3,4,5,6,7,10,11,12,13,14,16,17-tetradecahydro-cyclopenta[a]phenanthren-15-one

: 136203-70-8
(3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Guidance literature:: With potassium hydroxide; hydrazine hydrate; diethylene glycol; Yield given. Multistep reaction;
DOI:10.1248/cpb.39.1647

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 136203-70-8
(3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Guidance literature:: Multi-step reaction with 2 steps

2: 80percent hydrazine hydrate/diethylene glycol, 2) KOH

With potassium hydroxide; hydrazine hydrate; diethylene glycol;
DOI:10.1248/cpb.39.1647

Reference yield:

: 130257-78-2
2,2-Dimethyl-propionic acid (3S,5S,10S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-15-oxo-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

: 136203-70-8
(3S,5S,10S,13R,14S,17R)-14-Benzyloxymethyl-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,5,6,7,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-ol

Guidance literature:: Multi-step reaction with 2 steps

2: 80percent hydrazine hydrate/diethylene glycol, 2) KOH

With potassium hydroxide; hydrazine hydrate; diethylene glycol;
DOI:10.1248/cpb.39.1647