N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester

Base Information

Chemical Name:N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester
CAS No.:124227-54-9
Molecular Formula:C₂₆H₃₀N₂O₈S
Molecular Weight:530.599
Hs Code.:

<i>N</i>-(<i>N</i>-benzyloxycarbonyl-<i>O</i>-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-<i>S</i>-phenyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester

Chemical Property:

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Technology Process of N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester

There total 6 articles about N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115919-04-5
N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-L-glutamic acid-5-methyl ester

: 124227-54-9
N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester

Guidance literature:: With tetrahydrofuran; chloroformic acid ethyl ester; triethylamine; anschliessend Behandeln mit Thiophenol in THF;

Reference yield:

: 133525-29-8
N-(O-methyl-L-γ-glutamyl)-L-glutamic acid-5-methyl ester

: 124227-54-9
N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous KHCO₃; chlorocarbonic acid benzyl ester; diethyl ether

2: triethylamine; chlorocarbonic acid ethyl ester; THF / anschliessend Behandeln mit Thiophenol in THF

With tetrahydrofuran; diethyl ether; chloroformic acid ethyl ester; potassium hydrogencarbonate; benzyl chloroformate; triethylamine;

Reference yield:

: 4510-09-2
N-benzyloxycarbonyl-L-glutamic acid-5-hydrazide

: 124227-54-9
N-(N-benzyloxycarbonyl-O-methyl-L-γ-glutamyl)-1-thio-L-glutamic acid-5-methyl ester-S-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: diethyl ether; KHCO₃; H₂O

2: diazomethane; diethyl ether

3: palladium; aqueous methanol; acetic acid / Hydrogenation

4: aqueous KHCO₃; chlorocarbonic acid benzyl ester; diethyl ether

5: triethylamine; chlorocarbonic acid ethyl ester; THF / anschliessend Behandeln mit Thiophenol in THF

With tetrahydrofuran; diazomethane; methanol; diethyl ether; water; chloroformic acid ethyl ester; potassium hydrogencarbonate; palladium; acetic acid; benzyl chloroformate; triethylamine;