N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(S_P)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt

Base Information

• Chemical Name: N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(S_P)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt
• CAS No.: 142025-22-7
• Molecular Formula: C₆H₁₅N*C₅₈H₈₅N₁₀O₁₃PSSi₄
• Molecular Weight: 1406.95

Synonyms:

Chemical Property of N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(S_P)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt

Chemical Property:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(S_P)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt

There total 1 articles about N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(S_P)-P-thioadenylyl-(2'-5')-N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine (135732-99-9) + N6-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine-2'-(hydrogenphosphonate), triethylammonium salt (142025-16-9) → N6-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disilanediyl)-(SP)-P-thioadenylyl-(2'-5')-N6-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt (142025-22-7) + (RP)-N6-benzoyl-3'-O-(t.butyldimethylsilyl)-5'-O-(dimethoxytrityl)-P-thioadenylyl-(2'-5')-N6-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine, triethylammonium salt

Guidance literature:

With pyridine; pivaloyl chloride; sulfur; Yield given. Multistep reaction. Yields of byproduct given; 1) RT, 30 min;

DOI:10.1016/S0040-4020(01)92259-8

upstream raw materials:

N⁶-benzoyl-2',3'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine

N⁶-benzoyl-3',5'-O-(1,1,3,3-tetraisopropyl-1,3-disiloxanediyl)adenosine-2'-(hydrogenphosphonate), triethylammonium salt

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