2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate

Base Information

• Chemical Name: 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate
• CAS No.: 34564-45-9
• Molecular Formula: CH₃O₄S*C₂₈H₃₀N₅O₂S₃
• Molecular Weight: 675.875

Synonyms:

Chemical Property of 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate

There total 3 articles about 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3-ethyl-4-oxo-2-thioxothiazolidin-5-ylidenemethyl)-N-phenylacetamide (3747-06-6) → 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate (34564-45-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N, Py

2: (i), (ii) /BRN= 121471/, Py, Et₃N

With pyridine; triethylamine;

DOI:10.1007/BF00945517

Reference yield:

3,5-diethyl-2-methyl-1-phenyl-imidazo[4,5-c]pyridinediium; bis-(toluene-4-sulfonate) (35750-92-6) → 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate (34564-45-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N, Py

2: (i), (ii) /BRN= 121471/, Py, Et₃N

With pyridine; triethylamine;

DOI:10.1007/BF00945517

Reference yield:

3-ethylrhodanin (7648-01-3) + 3,5-diethyl-2-[2-(3-ethyl-4-oxo-2-thioxo-thiazolidin-5-ylidene)-ethylidene]-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; toluene-4-sulfonate (34564-44-8) + dimethyl sulfate (77-78-1) → 2-[2-(3,3'-diethyl-4,4'-dioxo-2'-thioxo-tetrahydro-[2,5']bithiazolylidene-5-ylidene)-ethylidene]-3,5-diethyl-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; methyl sulfate (34564-45-9)

Guidance literature:

Multistep reaction; (i), (ii) /BRN= 121471/, Py, Et₃N;

DOI:10.1007/BF00945517

upstream raw materials:

3-ethylrhodanin

3,5-diethyl-2-[2-(3-ethyl-4-oxo-2-thioxo-thiazolidin-5-ylidene)-ethylidene]-1-phenyl-2,3-dihydro-1H-imidazo[4,5-c]pyridinium; toluene-4-sulfonate

dimethyl sulfate

N-(3-ethyl-4-oxo-2-thioxothiazolidin-5-ylidenemethyl)-N-phenylacetamide

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