CuI₂[2-N-(phenyl)-dl-camphorquinoneimine]

Base Information

• Chemical Name: CuI₂[2-N-(phenyl)-dl-camphorquinoneimine]
• CAS No.: 81814-53-1
• Molecular Formula: C₁₆H₁₉CuI₂NO
• Molecular Weight: 558.688
• Mol file: 81814-53-1.mol

Synonyms:

Chemical Property of CuI₂[2-N-(phenyl)-dl-camphorquinoneimine]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of CuI₂[2-N-(phenyl)-dl-camphorquinoneimine]

There total 1 articles about CuI₂[2-N-(phenyl)-dl-camphorquinoneimine] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Camphorquinone (2767-84-2,10334-26-6,10373-78-1,71074-96-9,105309-30-6,465-29-2) + copper(II) iodide (13767-71-0) → CuI2[2-N-(phenyl)-dl-camphorquinoneimine] (81814-53-1) + CuI2[3-N-(phenyl)-dl-camphorquinoneimine] (81814-52-0)

Guidance literature:

With sodium acetate; aniline; In methanol; byproducts: 3-N-(phenyl)-dl-camphorquinoneimine, 2-N-(phenyl)-dl-camphorquinoneimine, 2,3-N-(phenyl)-dl-dl-camphorquinoneimine; methanolic soln. of metal salt was added to methanolic soln. of amine and dl-camphorquinone(metal:quinone:amine=1:2:4), methanolic susp. of NaOAc was added, stirred, reflux for 20 h on water bath; products not sepd., filtered at room temp., concd. in vac., org. product was extd. with n-hexane, residue extd. with C6H6 or CHCl3, soln. was concd. in vac., residue washed with n-hexane or C6H6, then 5-6 times withEt2O, elem. anal.;

upstream raw materials:

Camphorquinone

copper(II) iodide

Refernces