Benzene, 1,3,5-tris(chloromethyl)-2,4,6-triethyl-

Base Information

• Chemical Name: Benzene, 1,3,5-tris(chloromethyl)-2,4,6-triethyl-
• CAS No.: 142183-78-6
• Molecular Formula: C15H21Cl3
• Molecular Weight: 307.691
• DSSTox Substance ID: DTXSID60478529
• Nikkaji Number: J1.507.299G
• Wikidata: Q82311982
• Mol file: 142183-78-6.mol

Synonyms:Benzene, 1,3,5-tris(chloromethyl)-2,4,6-triethyl-;142183-78-6;SCHEMBL23092287;DTXSID60478529;1,3,5-tris(chloromethyl)-2,4,6-triethylbenzene

Chemical Property of Benzene, 1,3,5-tris(chloromethyl)-2,4,6-triethyl-

Chemical Property:

• XLogP3: 5.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 6
• Exact Mass: 306.070884
• Heavy Atom Count: 18
• Complexity: 176

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1=C(C(=C(C(=C1CCl)CC)CCl)CC)CCl

Technology Process of Benzene, 1,3,5-tris(chloromethyl)-2,4,6-triethyl-

There total 2 articles about Benzene, 1,3,5-tris(chloromethyl)-2,4,6-triethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,3,5-triethylbenzene (102-25-0) + chloromethyl methyl ether (107-30-2) → 1,3,5-tris(chloromethyl)-2,4,6-triethylbenzene (142183-78-6)

Guidance literature:

With tin(IV) chloride; In carbon disulfide; Heating;

DOI:10.1055/s-2005-869963

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 1,3,5-tris(chloromethyl)-2,4,6-triethylbenzene (142183-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / AlCl₃ / 12 h / 0 - 20 °C

2: 90 percent / SnCl₄ / CS₂ / Heating

With aluminium trichloride; tin(IV) chloride; In carbon disulfide;

DOI:10.1055/s-2005-869963

Reference yield: 92.0%

2-(1H-pyrazol-3-yl)pyridine (75415-03-1,192777-54-1) + 1,3,5-tris(chloromethyl)-2,4,6-triethylbenzene (142183-78-6) → (3-(2-pyridyl)pyrazolylmethyl)3C6(ethyl)3 (1027638-66-9)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In toluene; at 90 ℃; for 7h;

DOI:10.1039/b713503c

upstream raw materials:

1,3,5-triethylbenzene

chloromethyl methyl ether

benzene

Downstream raw materials:

1,3,5-tris(cyanomethyl)-2,4,6-triethylbenzene

1,3,5-tris(azidomethyl)-2,4,6-triethylbenzene

1,3,5-tris(hydroxymethyl)-2,4,6-triethylbenzene

N,N,N',N',N'',N''-hexa[(2-pyridyl)methyl]-1,3,5-tris(aminomethyl)-2,4,6-triethylbenzene